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Standard Test Method for Sulfur in Automotive, Heating, and Jet Fuels by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry
Automatische name übersetzung:
Standard Test Method for Schwefel in Automotive, Heizung, und Jet Fuels von Monochromatic energiedispersive Röntgenfluoreszenz-Spektrometrie
NORM herausgegeben am 15.1.2012
Bezeichnung normen: ASTM D7220-12
Anmerkung: UNGÜLTIG
Ausgabedatum normen: 15.1.2012
SKU: NS-37909
Zahl der Seiten: 7
Gewicht ca.: 21 g (0.05 Pfund)
Land: Amerikanische technische Norm
Kategorie: Technische Normen ASTM
Keywords:
automotive fuel, diesel, gasoline, petroleum, polarization, spectrometry, sulfur, X-ray, Automotive engine fuels/oils, Fluorescence polarization, Spectrometry, Sulfur, XRF (X-ray fluorescence), ICS Number Code 75.160.20 (Liquid fuels)
Significance and Use | ||||||||||
This test method provides measurement of total sulfur in automotive, No. 2 heating, and jet fuels with a minimum of sample preparation. A typical analysis time is 180 to 360 s per sample. The quality of automotive, No. 2 heating, and jet fuel can be related to the amount of sulfur present. Knowledge of sulfur concentration is necessary for processing purposes. There are also regulations promulgated in federal, state, and local agencies that restrict the amount of sulfur present in some fuel. If this test method is applied to petroleum materials with matrices significantly different from the calibration materials specified in this test method, the cautions and recommendations in Section 6 should be observed when interpreting the results. |
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1. Scope | ||||||||||
1.1 This test method specifies an energy-dispersive X-ray fluorescence (EDXRF) method for the determination of total sulfur in automotive, No. 2 heating, and jet fuels with a concentration range of 3 to 942 mg/kg. 1.1.1 The pooled limit of quantitation of this test method as obtained by statistical analysis of inter laboratory test results is 3 mg/kg sulfur. 1.1.2 This test method is applicable to gasoline, oxygen enriched gasoline (RFG), diesel, diesel/biodiesel blends containing up to twenty volume percent biodiesel, kerosene, jet fuel, jet fuel/biodiesel blends containing up to five volume percent biodiesel and No. 2 home heating oil. 1.2 A fundamental assumption in this test method is that the standard and sample matrix is well matched. Matrix mismatch can be caused by C/H ratio differences between samples and standards or by the presence of other heteroatoms. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3.1 The preferred concentration units are mg/kg sulfur. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. |
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2. Referenced Documents | ||||||||||
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1.10.2010
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1.12.2012
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1.5.2011
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1.10.2010
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15.11.2013
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15.4.2012
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